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Pulse methods in 1D and 2D liquid-phase NMR

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Published by Academic Press in San Diego, Calif .
Written in English

Subjects:

  • Nuclear magnetic resonance spectroscopy.,
  • Nuclear magnetic resonance, Pulsed.

Book details:

Edition Notes

Includes bibliographies and index.

Other titlesPulse methods in one D and two D liquid-phase NMR.
Statementedited by Wallace S. Brey.
ContributionsBrey, Wallace S.
Classifications
LC ClassificationsQD96.N8 P85 1988
The Physical Object
Paginationx, 561 p. :
Number of Pages561
ID Numbers
Open LibraryOL2373156M
ISBN 100121331555
LC Control Number87001224

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Genre/Form: Gepulste NMR-Spektroskopie: Additional Physical Format: Online version: Pulse methods in 1D and 2D liquid-phase NMR. San Diego, Calif.: Academic Press, © PULSE PROGRAM CATALOGUE: I. 1D & 2D NMR EXPERIMENTS Teodor Parella Servei RMN, Universitat Autònoma de Barcelona E-mail: [email protected] Size: 2MB. Pulsed NMR is used in magnetic resonance imaging (MRI). Purcell and Bloch won the Nobel Prize in Physics in for NMR; more recently NMR was the subject of Nobel Prizes in Chem-istry in and We have both NMR setups in the advanced labs: one is a variation of the CWNMR method, and the other is a pulsed NMR system. Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary.

Introduction to 1D and 2D NMR Spectroscopy (1) Basics Lecturer: Weiguo Hu A Conte () [email protected] October 2 Content At a Glance – Introduction to 1D and 2D NMR Spectroscopy Experimentation – What’s happening in the spectrometer when you type commands – Lock and shim – 1D NMR – 2D NMR. Key 2D NMR methods, used to obtain the homo- and heteronuclear correlations, through bond and space interactions, as well as chemical exchange spectroscopy are described, along with examples. The discussion is supplemented with 23 well chosen problems and their solutions which greatly help in developing a deeper understanding and appreciation. Brey, W.S. (ed.) () Pulse Methods in 1D and 2D Liquid-Phase NMR (Academic, San Diego) Google Scholar Carrington, A. and McLachlan, A.D. () Introduction to Magnetic Resonance with Applications to Chemistry and Chemical Physics (Harper and Row, New York) Google Scholar.   Carbon NMR is a necessary step in full structural characterization. However, ¹³C-NMR alone does not provide enough information to assign the carbons in the molecule. The NMR spectrum below does confirm the number of carbons in the molecule; however, HSQC and HMBC (we will get to these soon!) are necessary to assign the carbons with confidence.

1. Author(s): Brey,Wallace S Title(s): Pulse methods in 1D and 2D liquid-phase NMR/ edited by Wallace S. Brey. Country of Publication: United States Publisher: San Diego, Calif.: . Cite this chapter as: Bodenhausen G. () Various Operator Formalisms for the Description of Pulse Methods in NMR. In: Granger P., Harris R.K. (eds) Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications. Experiment - 17O NMR Spectroscopy with RIDE 75 Experiment - 47/49Ti NMR Spectroscopy with ARING 76 CHAPTER 10 - THE SECOND DIMENSION 77 SUMMARY 77 Experiment - 2D J-Resolved 1H NMR Spectroscopy 77 Experiment - 2D J-Resolved 13C NMR Spectroscopy 78 Experiment - The Basic H,H-COSY-Experiment 79 Experiment - Long-Range. P(i) Pulse width; PL(i) ; PLW(i) or PLdb(i) Pulse power level e.g. Bruker Convention P1 90 degree pulse for nucleus to be detected. PL1 the corresponding power to obtain the 90 degree for maximum signal. Soft pulses: Shape pulse (e.g. used in Solvent suppression and 1D NOE). Gradient pulse (e.g. used in most 1D and 2D NMR measurements).